Information card for entry 7121458

Structure parameters

• Chemical name: [{pinBO(py)UOU(py)OBpin}(LA)]
• Formula: C94 H98 B2 N10 O7 U2
• Calculated formula: C93.9994 H98 B2 N10 O7 U2
• Title of publication: Double uranium oxo cations derived from uranyl by borane or silane reduction.
• Authors of publication: Cowie, Bradley E.; Nichol, Gary S.; Love, Jason B.; Arnold, Polly L.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 31
• Pages of publication: 3839 - 3842
• a: 14.7593 ± 0.0005 Å
• b: 15.6981 ± 0.0006 Å
• c: 20.1394 ± 0.0007 Å
• α: 74.615 ± 0.002°
• β: 87.841 ± 0.002°
• γ: 69.604 ± 0.002°
• Cell volume: 4209.1 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0335
• Residual factor for significantly intense reflections: 0.0248
• Weighted residual factors for significantly intense reflections: 0.0516
• Weighted residual factors for all reflections included in the refinement: 0.0568
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No