Information card for entry 7121459

Structure parameters

• Chemical name: [{(py){cat(py)BO)UOUOBcat(py)}(LA)]
• Formula: C89 H79 B2 N11 O8 U2
• Calculated formula: C89 H79 B2 N11 O8 U2
• Title of publication: Double uranium oxo cations derived from uranyl by borane or silane reduction.
• Authors of publication: Cowie, Bradley E.; Nichol, Gary S.; Love, Jason B.; Arnold, Polly L.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 31
• Pages of publication: 3839 - 3842
• a: 14.8167 ± 0.0003 Å
• b: 15.0681 ± 0.0003 Å
• c: 18.9308 ± 0.0004 Å
• α: 68.593 ± 0.001°
• β: 79.072 ± 0.001°
• γ: 86.228 ± 0.001°
• Cell volume: 3863.52 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0519
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0586
• Weighted residual factors for all reflections included in the refinement: 0.0649
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No