Information card for entry 7121461

Structure parameters

• Chemical name: [{HPh2SiO(py)UOU(py)OSiPh2H}(LA)]
• Formula: C97 H85 N11 O3 Si2 U2
• Calculated formula: C97 H85 N11 O3 Si2 U2
• Title of publication: Double uranium oxo cations derived from uranyl by borane or silane reduction.
• Authors of publication: Cowie, Bradley E.; Nichol, Gary S.; Love, Jason B.; Arnold, Polly L.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 31
• Pages of publication: 3839 - 3842
• a: 23.8381 ± 0.0005 Å
• b: 17.7807 ± 0.0002 Å
• c: 21.4711 ± 0.0004 Å
• α: 90°
• β: 114.099 ± 0.002°
• γ: 90°
• Cell volume: 8307.5 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0406
• Residual factor for significantly intense reflections: 0.0302
• Weighted residual factors for significantly intense reflections: 0.0907
• Weighted residual factors for all reflections included in the refinement: 0.0994
• Goodness-of-fit parameter for all reflections included in the refinement: 0.766
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No