Information card for entry 7121460

Structure parameters

• Chemical name: [{HPh2SiO(THF)UOU(THF)OSiPh2H}(LA)]
• Formula: C98 H102 N8 O7 Si2 U2
• Calculated formula: C98 H102 N8 O7 Si2 U2
• Title of publication: Double uranium oxo cations derived from uranyl by borane or silane reduction.
• Authors of publication: Cowie, Bradley E.; Nichol, Gary S.; Love, Jason B.; Arnold, Polly L.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 31
• Pages of publication: 3839 - 3842
• a: 22.5124 ± 0.0002 Å
• b: 19.8405 ± 0.0002 Å
• c: 20.141 ± 0.0002 Å
• α: 90°
• β: 110.283 ± 0.001°
• γ: 90°
• Cell volume: 8438.29 ± 0.15 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0267
• Weighted residual factors for significantly intense reflections: 0.0538
• Weighted residual factors for all reflections included in the refinement: 0.0574
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No