Crystallography Open Database

Information card for entry 7122055

7122054 << 7122055 >> 7122056

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Coordinates	7122055.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H66 Cl N5 Ni O5 Si2
Calculated formula	C39 H66 Cl N5 Ni O5 Si2
Title of publication	Metal nitrene-like reactivity of a Si[double bond, length as m-dash]N bond towards CO<sub>2</sub>.
Authors of publication	Hadlington, Terrance J.; Szilvási, Tibor; Driess, Matthias
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	67
Pages of publication	9352 - 9355
a	9.394 ± 0.0005 Å
b	11.9351 ± 0.0006 Å
c	20.7497 ± 0.0011 Å
α	86.519 ± 0.004°
β	79.694 ± 0.004°
γ	82.07 ± 0.004°
Cell volume	2265.4 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	1
Hermann-Mauguin space group symbol	P 1
Hall space group symbol	P 1
Residual factor for all reflections	0.0938
Residual factor for significantly intense reflections	0.0739
Weighted residual factors for significantly intense reflections	0.1836
Weighted residual factors for all reflections included in the refinement	0.2067
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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