Information card for entry 7122142

Structure parameters

• Formula: C19 H19 N O2
• Calculated formula: C19 H19 N O2
• Title of publication: A photocatalytic iminyl radical-mediated C-C bond cleavage/addition/cyclization cascade for the synthesis of 1,2,3,4-tetrahydrophenanthrenes.
• Authors of publication: Wang, Peng-Zi; Yu, Xiao-Ye; Li, Chan-Yun; He, Bin-Qing; Chen, Jia-Rong; Xiao, Wen-Jing
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 71
• Pages of publication: 9925 - 9928
• a: 7.7693 ± 0.0013 Å
• b: 12.582 ± 0.002 Å
• c: 15.723 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1537 ± 0.5 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273.15 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0621
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.1123
• Weighted residual factors for all reflections included in the refinement: 0.1223
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No