Information card for entry 7122143
| Formula |
C21 H21 N O4 |
| Calculated formula |
C21 H21 N O4 |
| Title of publication |
A photocatalytic iminyl radical-mediated C-C bond cleavage/addition/cyclization cascade for the synthesis of 1,2,3,4-tetrahydrophenanthrenes. |
| Authors of publication |
Wang, Peng-Zi; Yu, Xiao-Ye; Li, Chan-Yun; He, Bin-Qing; Chen, Jia-Rong; Xiao, Wen-Jing |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2018 |
| Journal volume |
54 |
| Journal issue |
71 |
| Pages of publication |
9925 - 9928 |
| a |
10.271 ± 0.002 Å |
| b |
18.417 ± 0.004 Å |
| c |
10.492 ± 0.002 Å |
| α |
90° |
| β |
114.416 ± 0.003° |
| γ |
90° |
| Cell volume |
1807.2 ± 0.6 Å3 |
| Cell temperature |
296 ± 2 K |
| Ambient diffraction temperature |
296 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/n 1 |
| Hall space group symbol |
-P 2yn |
| Residual factor for all reflections |
0.1015 |
| Residual factor for significantly intense reflections |
0.0561 |
| Weighted residual factors for significantly intense reflections |
0.1602 |
| Weighted residual factors for all reflections included in the refinement |
0.1898 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.03 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7122143.html
