Information card for entry 7122456

Structure parameters

• Formula: C34 H44 N4 O4
• Calculated formula: C34 H44 N4 O4
• Title of publication: Catalytic enantioselective ene-type reactions of vinylogous hydrazone: construction of α-methylene-γ-butyrolactone derivatives.
• Authors of publication: Zhang, Hang; Yao, Qian; Cao, Weidi; Ge, Shulin; Xu, Jinxiu; Liu, Xiaohua; Feng, Xiaoming
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 88
• Pages of publication: 12511 - 12514
• a: 8.1154 ± 0.0011 Å
• b: 9.9402 ± 0.0013 Å
• c: 10.784 ± 0.0014 Å
• α: 78.245 ± 0.005°
• β: 87.577 ± 0.006°
• γ: 69.347 ± 0.005°
• Cell volume: 796.54 ± 0.18 ų
• Cell temperature: 300 ± 2 K
• Ambient diffraction temperature: 300 ± 2 K
• Number of distinct elements: 4
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0346
• Residual factor for significantly intense reflections: 0.0324
• Weighted residual factors for significantly intense reflections: 0.0836
• Weighted residual factors for all reflections included in the refinement: 0.0861
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No