Information card for entry 7122457

Structure parameters

• Formula: C50 H74 F12 N8 O13 S4 Zn
• Calculated formula: C50 H74 F12 N8 O13 S4 Zn
• Title of publication: Catalytic enantioselective ene-type reactions of vinylogous hydrazone: construction of α-methylene-γ-butyrolactone derivatives.
• Authors of publication: Zhang, Hang; Yao, Qian; Cao, Weidi; Ge, Shulin; Xu, Jinxiu; Liu, Xiaohua; Feng, Xiaoming
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 88
• Pages of publication: 12511 - 12514
• a: 20.73104 ± 0.00017 Å
• b: 15.56761 ± 0.00012 Å
• c: 24.0468 ± 0.0002 Å
• α: 90°
• β: 103.086 ± 0.0009°
• γ: 90°
• Cell volume: 7559.15 ± 0.11 ų
• Cell temperature: 140.2 ± 0.2 K
• Ambient diffraction temperature: 140.2 ± 0.2 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0688
• Residual factor for significantly intense reflections: 0.0633
• Weighted residual factors for significantly intense reflections: 0.1708
• Weighted residual factors for all reflections included in the refinement: 0.1774
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No