Information card for entry 7122460

Structure parameters

• Formula: C36 H54 N77 Ni10 O15 Y
• Calculated formula: C36 H54 N77 Ni10 O15 Y
• Title of publication: Increasing the nuclearity and spin ground state in a new family of ferromagnetically-coupled {Ni₁₀} disk-like complexes bearing exclusively end-on bridging azido ligands.
• Authors of publication: Krause, Jasmin; Alexandropoulos, Dimitris I.; Carrella, Luca M.; Rentschler, Eva; Stamatatos, Theocharis C.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 88
• Pages of publication: 12499 - 12502
• a: 11.0684 ± 0.0012 Å
• b: 14.2915 ± 0.0016 Å
• c: 16.0071 ± 0.0014 Å
• α: 78.715 ± 0.009°
• β: 84.321 ± 0.008°
• γ: 81.693 ± 0.009°
• Cell volume: 2450.5 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173.15 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1195
• Residual factor for significantly intense reflections: 0.0537
• Weighted residual factors for significantly intense reflections: 0.1177
• Weighted residual factors for all reflections included in the refinement: 0.1482
• Goodness-of-fit parameter for all reflections included in the refinement: 0.85
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No