Information card for entry 7122461

Structure parameters

• Formula: C36 H54 N77 Ni10 O17 Tb
• Calculated formula: C36 H54 N77 Ni10 O17 Tb
• Title of publication: Increasing the nuclearity and spin ground state in a new family of ferromagnetically-coupled {Ni₁₀} disk-like complexes bearing exclusively end-on bridging azido ligands.
• Authors of publication: Krause, Jasmin; Alexandropoulos, Dimitris I.; Carrella, Luca M.; Rentschler, Eva; Stamatatos, Theocharis C.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 88
• Pages of publication: 12499 - 12502
• a: 11.16 ± 0.002 Å
• b: 19.509 ± 0.004 Å
• c: 23.698 ± 0.004 Å
• α: 106.432 ± 0.004°
• β: 91.339 ± 0.004°
• γ: 94.085 ± 0.004°
• Cell volume: 4931.1 ± 1.6 ų
• Cell temperature: 173.15 ± 0.02 K
• Ambient diffraction temperature: 173.15 ± 0.02 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1362
• Residual factor for significantly intense reflections: 0.0652
• Weighted residual factors for significantly intense reflections: 0.1353
• Weighted residual factors for all reflections included in the refinement: 0.1641
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No