Information card for entry 7122927

Structure parameters

• Formula: C10 H29 B10 P3
• Calculated formula: C10 H29 B10 P3
• Title of publication: Molecular Doping: Accessing the First Carborane-substituted 1,2,3-Triphospholanide via Insertion of P− into a P−P bond
• Authors of publication: Hey-Hawkins, Evamarie; Coburger, Peter; Gruetzmacher, Hansjoerg
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 9.9771 ± 0.0004 Å
• b: 21.9776 ± 0.0007 Å
• c: 10.192 ± 0.0004 Å
• α: 90°
• β: 117.372 ± 0.005°
• γ: 90°
• Cell volume: 1984.62 ± 0.16 ų
• Cell temperature: 130 K
• Ambient diffraction temperature: 130 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0905
• Residual factor for significantly intense reflections: 0.0672
• Weighted residual factors for significantly intense reflections: 0.159
• Weighted residual factors for all reflections included in the refinement: 0.1705
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No