Information card for entry 7122928

Structure parameters

• Formula: C10.8 H25.6 B8 Cl0.8 P2.4
• Calculated formula: C10.8 H25.6 B8 Cl0.8 P2.4
• Title of publication: Molecular Doping: Accessing the First Carborane-substituted 1,2,3-Triphospholanide via Insertion of P− into a P−P bond
• Authors of publication: Hey-Hawkins, Evamarie; Coburger, Peter; Gruetzmacher, Hansjoerg
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 28.5977 ± 0.0009 Å
• b: 12.051 ± 0.0005 Å
• c: 16.6081 ± 0.0005 Å
• α: 90°
• β: 124.396 ± 0.003°
• γ: 90°
• Cell volume: 4722.9 ± 0.3 ų
• Cell temperature: 130 K
• Ambient diffraction temperature: 130 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0714
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.0929
• Weighted residual factors for all reflections included in the refinement: 0.1047
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No