Information card for entry 7123859

Structure parameters

• Formula: C33.5 H70 Cl Fe Ge2 N5 O3 Si2
• Calculated formula: C33.5 H70 Cl Fe Ge2 N5 O3 Si2
• Title of publication: Symmetric and non-symmetric bis-metallylene iron complexes, precursors of iron germanide nanoparticles
• Authors of publication: Sodreau, Alexandre; Lentz, Nicolas; Frutos, Maria; Ladeira, Sonia; Nayral, Celine; Delpech, Fabien; Madec, David
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 44.814 ± 0.002 Å
• b: 9.9093 ± 0.0004 Å
• c: 21.2706 ± 0.001 Å
• α: 90°
• β: 107.296 ± 0.002°
• γ: 90°
• Cell volume: 9018.6 ± 0.7 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0644
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections included in the refinement: 0.1158
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No