Information card for entry 7123860

Structure parameters

• Formula: C44 H92 Cl4 N8 O2 Sn4
• Calculated formula: C44 H92 Cl4 N8 O2 Sn4
• Title of publication: Symmetric and non-symmetric bis-metallylene iron complexes, precursors of iron germanide nanoparticles
• Authors of publication: Sodreau, Alexandre; Lentz, Nicolas; Frutos, Maria; Ladeira, Sonia; Nayral, Celine; Delpech, Fabien; Madec, David
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 9.9149 ± 0.0004 Å
• b: 18.3126 ± 0.0008 Å
• c: 16.2508 ± 0.0007 Å
• α: 90°
• β: 104.495 ± 0.002°
• γ: 90°
• Cell volume: 2856.7 ± 0.2 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0594
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.1098
• Weighted residual factors for all reflections included in the refinement: 0.1522
• Goodness-of-fit parameter for all reflections included in the refinement: 1.202
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No