Information card for entry 7125438

Structure parameters

• Formula: C23 H26 Au B Cl N7 O2 W
• Calculated formula: C23 H26 Au B Cl N7 O2 W
• Title of publication: Synthesis of pyridyl carbyne complexes and their conversion to N-heterocyclic vinylidenes
• Authors of publication: Hill, Anthony; Frogley, Benjamin
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 15.8904 ± 0.0003 Å
• b: 9.6054 ± 0.0002 Å
• c: 17.1964 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2624.75 ± 0.09 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0391
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.0971
• Weighted residual factors for all reflections included in the refinement: 0.0984
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No