Information card for entry 7125439

Structure parameters

• Formula: C25 H30 B Cl2 N7 O2 Pt W
• Calculated formula: C25 H30 B Cl2 N7 O2 Pt W
• Title of publication: Synthesis of pyridyl carbyne complexes and their conversion to N-heterocyclic vinylidenes
• Authors of publication: Hill, Anthony; Frogley, Benjamin
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 10.6485 ± 0.0004 Å
• b: 21.1039 ± 0.0009 Å
• c: 13.1797 ± 0.0005 Å
• α: 90°
• β: 91.758 ± 0.004°
• γ: 90°
• Cell volume: 2960.4 ± 0.2 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0533
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.0834
• Weighted residual factors for all reflections included in the refinement: 0.0892
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No