Information card for entry 7125961

Structure parameters

• Formula: C42 H64 N4 Na O4
• Calculated formula: C42 H64 N4 Na O4
• Title of publication: Stable, yet "naked", azo radical anion ArNNAr^- and dianion ArNNAr^2- (Ar = 4-CN-2,6-ⁱPr₂-C₆H₂) with selective CO₂ activation.
• Authors of publication: Wang, Wenqing; Tan, Gengwen; Feng, Rui; Fang, Yong; Chen, Chao; Ruan, Huapeng; Zhao, Yue; Wang, Xinping
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 22
• Pages of publication: 3285 - 3288
• a: 18.399 ± 0.002 Å
• b: 14.6911 ± 0.0016 Å
• c: 15.7048 ± 0.0016 Å
• α: 90°
• β: 103.277 ± 0.003°
• γ: 90°
• Cell volume: 4131.6 ± 0.8 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0901
• Residual factor for significantly intense reflections: 0.0666
• Weighted residual factors for significantly intense reflections: 0.1712
• Weighted residual factors for all reflections included in the refinement: 0.1903
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No