Information card for entry 7125962

Structure parameters

• Formula: C42 H64 K N4 O4
• Calculated formula: C42 H63.998 K N4 O4
• Title of publication: Stable, yet "naked", azo radical anion ArNNAr^- and dianion ArNNAr^2- (Ar = 4-CN-2,6-ⁱPr₂-C₆H₂) with selective CO₂ activation.
• Authors of publication: Wang, Wenqing; Tan, Gengwen; Feng, Rui; Fang, Yong; Chen, Chao; Ruan, Huapeng; Zhao, Yue; Wang, Xinping
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 22
• Pages of publication: 3285 - 3288
• a: 18.731 ± 0.004 Å
• b: 15.129 ± 0.003 Å
• c: 15.467 ± 0.003 Å
• α: 90°
• β: 104.882 ± 0.004°
• γ: 90°
• Cell volume: 4236 ± 1.5 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.107
• Residual factor for significantly intense reflections: 0.077
• Weighted residual factors for significantly intense reflections: 0.1914
• Weighted residual factors for all reflections included in the refinement: 0.215
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No