Information card for entry 7128702

Structure parameters

• Formula: C86 H115 K N4 O5 V
• Calculated formula: C86 H115 K N4 O5 V
• Title of publication: Systematic reductive oligomerization of isocyanides with a vanadium(ii) complex.
• Authors of publication: Hasegawa, Sui; Ishida, Yutaka; Kawaguchi, Hiroyuki
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 67
• Pages of publication: 8296 - 8299
• a: 13.4233 ± 0.0003 Å
• b: 16.9491 ± 0.0004 Å
• c: 19.8449 ± 0.0004 Å
• α: 67.448 ± 0.002°
• β: 81.026 ± 0.002°
• γ: 69.914 ± 0.002°
• Cell volume: 3914.57 ± 0.17 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0817
• Residual factor for significantly intense reflections: 0.0591
• Weighted residual factors for significantly intense reflections: 0.1559
• Weighted residual factors for all reflections included in the refinement: 0.1717
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No