Crystallography Open Database

Information card for entry 7128703

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Coordinates	7128703.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H94 K N5 O4 V
Calculated formula	C65 H94 K N5 O4 V
Title of publication	Systematic reductive oligomerization of isocyanides with a vanadium(ii) complex.
Authors of publication	Hasegawa, Sui; Ishida, Yutaka; Kawaguchi, Hiroyuki
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2021
Journal volume	57
Journal issue	67
Pages of publication	8296 - 8299
a	39.7195 ± 0.0002 Å
b	17.1396 ± 0.0001 Å
c	18.6902 ± 0.0001 Å
α	90°
β	93.079 ± 0.001°
γ	90°
Cell volume	12705.5 ± 0.12 Å³
Cell temperature	123 K
Ambient diffraction temperature	123 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.039
Residual factor for significantly intense reflections	0.0363
Weighted residual factors for significantly intense reflections	0.1006
Weighted residual factors for all reflections included in the refinement	0.1026
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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