Information card for entry 7128704

Structure parameters

• Formula: C48 H69 K N2 O4 Si V
• Calculated formula: C48 H69 K N2 O4 Si V
• Title of publication: Systematic reductive oligomerization of isocyanides with a vanadium(ii) complex.
• Authors of publication: Hasegawa, Sui; Ishida, Yutaka; Kawaguchi, Hiroyuki
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 67
• Pages of publication: 8296 - 8299
• a: 14.2203 ± 0.0004 Å
• b: 22.6239 ± 0.0007 Å
• c: 15.3959 ± 0.0004 Å
• α: 90°
• β: 96.58 ± 0.002°
• γ: 90°
• Cell volume: 4920.5 ± 0.2 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0661
• Residual factor for significantly intense reflections: 0.0465
• Weighted residual factors for significantly intense reflections: 0.1014
• Weighted residual factors for all reflections included in the refinement: 0.1107
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No