Information card for entry 7132515

Structure parameters

• Formula: C104 H148 K2 Mg2 N4 O2
• Calculated formula: C104 H148 K2 Mg2 N4 O2
• Title of publication: Steric control of Mg-Mg bond formation <i>vs.</i> N₂ activation in the reduction of bulky magnesium diamide complexes.
• Authors of publication: Mondal, Rahul; Evans, Matthew J.; Nguyen, Dat T.; Rajeshkumar, Thayalan; Maron, Laurent; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 8
• Pages of publication: 1016 - 1019
• a: 16.5142 ± 0.0003 Å
• b: 16.8828 ± 0.0003 Å
• c: 17.9517 ± 0.0003 Å
• α: 90.877 ± 0.002°
• β: 90.703 ± 0.002°
• γ: 106.972 ± 0.002°
• Cell volume: 4785.76 ± 0.15 ų
• Cell temperature: 123.01 ± 0.1 K
• Ambient diffraction temperature: 123.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0971
• Residual factor for significantly intense reflections: 0.0825
• Weighted residual factors for significantly intense reflections: 0.2127
• Weighted residual factors for all reflections included in the refinement: 0.2274
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No