Information card for entry 7132516

Structure parameters

• Formula: C113 H168 K2 Mg2 N4 O2
• Calculated formula: C113 H168 K2 Mg2 N4 O2
• Title of publication: Steric control of Mg-Mg bond formation <i>vs.</i> N₂ activation in the reduction of bulky magnesium diamide complexes.
• Authors of publication: Mondal, Rahul; Evans, Matthew J.; Nguyen, Dat T.; Rajeshkumar, Thayalan; Maron, Laurent; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 8
• Pages of publication: 1016 - 1019
• a: 17.4631 ± 0.0004 Å
• b: 18.269 ± 0.0003 Å
• c: 19.28 ± 0.0003 Å
• α: 102.56 ± 0.002°
• β: 105.43 ± 0.002°
• γ: 92.826 ± 0.002°
• Cell volume: 5749.7 ± 0.2 ų
• Cell temperature: 123.01 ± 0.1 K
• Ambient diffraction temperature: 123.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1254
• Residual factor for significantly intense reflections: 0.0959
• Weighted residual factors for significantly intense reflections: 0.2554
• Weighted residual factors for all reflections included in the refinement: 0.2782
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No