Information card for entry 7132517

Structure parameters

• Formula: C103 H144 K2 Mg2 N4 O3
• Calculated formula: C103 H144 K2 Mg2 N4 O3
• Title of publication: Steric control of Mg-Mg bond formation <i>vs.</i> N₂ activation in the reduction of bulky magnesium diamide complexes.
• Authors of publication: Mondal, Rahul; Evans, Matthew J.; Nguyen, Dat T.; Rajeshkumar, Thayalan; Maron, Laurent; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 8
• Pages of publication: 1016 - 1019
• a: 18.1842 ± 0.0001 Å
• b: 22.1675 ± 0.0001 Å
• c: 24.5607 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9900.38 ± 0.08 ų
• Cell temperature: 123 ± 0.1 K
• Ambient diffraction temperature: 123 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0464
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.1225
• Weighted residual factors for all reflections included in the refinement: 0.1266
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No