Information card for entry 7133143

Structure parameters

• Formula: C149 H136 B2 F48 N4 O6 P2
• Calculated formula: C149 H136 B2 F48 N4 O6 P2
• Title of publication: P(V)-bis(amidophenolate) ligand cooperation: stoichiometric CO-bond cleavage in aldehydes and ketones.
• Authors of publication: Karnbrock, Simon B. H.; Golz, Christopher; Alcarazo, Manuel
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 53
• Pages of publication: 6745 - 6748
• a: 13.6399 ± 0.0013 Å
• b: 16.8477 ± 0.0013 Å
• c: 19.2953 ± 0.0016 Å
• α: 115.857 ± 0.003°
• β: 102.316 ± 0.002°
• γ: 98.273 ± 0.002°
• Cell volume: 3754.1 ± 0.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0683
• Residual factor for significantly intense reflections: 0.0531
• Weighted residual factors for significantly intense reflections: 0.1336
• Weighted residual factors for all reflections included in the refinement: 0.1474
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No