Information card for entry 7133144

Structure parameters

• Formula: C45 H60 Cl7 Ga2 N2 O3 P
• Calculated formula: C45 H60 Cl7 Ga2 N2 O3 P
• Title of publication: P(V)-bis(amidophenolate) ligand cooperation: stoichiometric CO-bond cleavage in aldehydes and ketones.
• Authors of publication: Karnbrock, Simon B. H.; Golz, Christopher; Alcarazo, Manuel
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 53
• Pages of publication: 6745 - 6748
• a: 20.964 ± 0.0007 Å
• b: 12.2176 ± 0.0003 Å
• c: 20.1457 ± 0.0007 Å
• α: 90°
• β: 93.743 ± 0.001°
• γ: 90°
• Cell volume: 5148.9 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0231
• Residual factor for significantly intense reflections: 0.0224
• Weighted residual factors for significantly intense reflections: 0.058
• Weighted residual factors for all reflections included in the refinement: 0.0583
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No