Information card for entry 7133261

Structure parameters

• Formula: C144 H212 K2 N2 O26 Ti2
• Calculated formula: C130 H190 K2 N2 O24 Ti2
• Title of publication: Hydrazido complexes prepared by methylation of an anionic end-on bridging dinitrogen dititanium complex.
• Authors of publication: Ishida, Yutaka; Nakanishi, Yusuke; Hiratsuka, Takuma; Kawaguchi, Hiroyuki
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 58
• Pages of publication: 7459 - 7462
• a: 13.452 ± 0.0004 Å
• b: 22.8729 ± 0.0007 Å
• c: 23.7434 ± 0.0008 Å
• α: 101.621 ± 0.003°
• β: 94.411 ± 0.003°
• γ: 90.086 ± 0.003°
• Cell volume: 7133.5 ± 0.4 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2061
• Residual factor for significantly intense reflections: 0.0907
• Weighted residual factors for significantly intense reflections: 0.1916
• Weighted residual factors for all reflections included in the refinement: 0.2396
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No