Crystallography Open Database

Information card for entry 7133262

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Coordinates	7133262.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C108 H158 K2 N2 O10 Ti2
Calculated formula	C108 H158 K2 N2 O10 Ti2
Title of publication	Hydrazido complexes prepared by methylation of an anionic end-on bridging dinitrogen dititanium complex.
Authors of publication	Ishida, Yutaka; Nakanishi, Yusuke; Hiratsuka, Takuma; Kawaguchi, Hiroyuki
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	58
Pages of publication	7459 - 7462
a	13.92 ± 0.0001 Å
b	25.4342 ± 0.0002 Å
c	30.2821 ± 0.0002 Å
α	90°
β	103.153 ± 0.001°
γ	90°
Cell volume	10439.9 ± 0.14 Å³
Cell temperature	123 K
Ambient diffraction temperature	123 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0438
Residual factor for significantly intense reflections	0.0422
Weighted residual factors for significantly intense reflections	0.1134
Weighted residual factors for all reflections included in the refinement	0.1148
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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