Information card for entry 7133464

Structure parameters

• Formula: C18 H34 Al4 N2 O2
• Calculated formula: C18 H34 Al4 N2 O2
• Title of publication: Controlled hydrolysis of AlMe₃ to tetramethylalumoxane and a new look at incipient adducts with water.
• Authors of publication: Korona, Krzesimir; Justyniak, Iwona; Pogrebetsky, James; Lemieszka, Marta; Bernatowicz, Piotr; Pietrzykowski, Antoni; Kubas, Adam; Lewiński, Janusz
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 70
• Pages of publication: 9392 - 9395
• a: 8.359 ± 0.0003 Å
• b: 8.9229 ± 0.0003 Å
• c: 9.209 ± 0.0003 Å
• α: 99.654 ± 0.003°
• β: 111.823 ± 0.003°
• γ: 91.082 ± 0.003°
• Cell volume: 626.13 ± 0.04 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0342
• Residual factor for significantly intense reflections: 0.0334
• Weighted residual factors for significantly intense reflections: 0.0923
• Weighted residual factors for all reflections included in the refinement: 0.0928
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No