Information card for entry 7133465

Structure parameters

• Formula: C22 H44 Al4 N4 O2
• Calculated formula: C22 H44 Al4 N4 O2
• Title of publication: Controlled hydrolysis of AlMe₃ to tetramethylalumoxane and a new look at incipient adducts with water.
• Authors of publication: Korona, Krzesimir; Justyniak, Iwona; Pogrebetsky, James; Lemieszka, Marta; Bernatowicz, Piotr; Pietrzykowski, Antoni; Kubas, Adam; Lewiński, Janusz
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 70
• Pages of publication: 9392 - 9395
• a: 8.118 ± 0.0004 Å
• b: 13.749 ± 0.0006 Å
• c: 14.0249 ± 0.0004 Å
• α: 86.298 ± 0.003°
• β: 77.725 ± 0.003°
• γ: 73.794 ± 0.004°
• Cell volume: 1468.79 ± 0.11 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0461
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.1025
• Weighted residual factors for all reflections included in the refinement: 0.1044
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No