Crystallography Open Database

Information card for entry 7135403

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Coordinates	7135403.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H14 Ge0.5 N3
Calculated formula	C16 H14 Ge0.5 N3
Title of publication	Anilido-pyrazole ligand supported germylenes: synthesis, structure, and catalytic <i>N</i>-formylation of amines using CO<sub>2</sub>.
Authors of publication	Barik, Jogendrananda; Rit, Arnab
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2026
Journal volume	62
Journal issue	13
Pages of publication	4131 - 4134
a	18.5498 ± 0.0014 Å
b	7.608 ± 0.0007 Å
c	18.5459 ± 0.0017 Å
α	90°
β	93.523 ± 0.003°
γ	90°
Cell volume	2612.4 ± 0.4 Å³
Cell temperature	167 ± 2 K
Ambient diffraction temperature	167 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0434
Residual factor for significantly intense reflections	0.0423
Weighted residual factors for significantly intense reflections	0.1269
Weighted residual factors for all reflections included in the refinement	0.1277
Goodness-of-fit parameter for all reflections included in the refinement	1.181
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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