Information card for entry 7135404

Structure parameters

• Formula: C3.38 H4.92 Ge0.15 N0.62 Si0.31
• Calculated formula: C3.38462 H4.92308 Ge0.153846 N0.615385 Si0.307692
• Title of publication: Anilido-pyrazole ligand supported germylenes: synthesis, structure, and catalytic <i>N</i>-formylation of amines using CO₂.
• Authors of publication: Barik, Jogendrananda; Rit, Arnab
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2026
• Journal volume: 62
• Journal issue: 13
• Pages of publication: 4131 - 4134
• a: 9.2899 ± 0.0005 Å
• b: 13.6579 ± 0.0009 Å
• c: 19.1626 ± 0.0013 Å
• α: 90°
• β: 102.816 ± 0.002°
• γ: 90°
• Cell volume: 2370.8 ± 0.3 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0239
• Residual factor for significantly intense reflections: 0.0218
• Weighted residual factors for significantly intense reflections: 0.063
• Weighted residual factors for all reflections included in the refinement: 0.064
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No