Synthesis of a family of 3-alkyl- or 3-aryl-substituted 1,2-dihydroquinazolinium salts and their isomerization to 4-iminium-1,2,3,4-tetrahydroquinolines.
Authors of publication
Vicente, José; Chicote, María Teresa; Martínez-Martínez, Antonio Jesús; Bautista, Delia; Jones, Peter G.
Journal of publication
Organic & biomolecular chemistry
Year of publication
2011
Journal volume
9
Journal issue
7
Pages of publication
2279 - 2285
a
13.531 ± 0.002 Å
b
17.185 ± 0.002 Å
c
19.511 ± 0.002 Å
α
108.267 ± 0.013°
β
106.724 ± 0.013°
γ
101.091 ± 0.014°
Cell volume
3921.8 ± 1.1 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0942
Residual factor for significantly intense reflections
0.0613
Weighted residual factors for significantly intense reflections
0.1666
Weighted residual factors for all reflections included in the refinement
0.1843
Goodness-of-fit parameter for all reflections included in the refinement
