Synthesis of a family of 3-alkyl- or 3-aryl-substituted 1,2-dihydroquinazolinium salts and their isomerization to 4-iminium-1,2,3,4-tetrahydroquinolines.
Authors of publication
Vicente, José; Chicote, María Teresa; Martínez-Martínez, Antonio Jesús; Bautista, Delia; Jones, Peter G.
Journal of publication
Organic & biomolecular chemistry
Year of publication
2011
Journal volume
9
Journal issue
7
Pages of publication
2279 - 2285
a
11.8166 ± 0.0017 Å
b
16.328 ± 0.002 Å
c
13.928 ± 0.002 Å
α
90°
β
102.356 ± 0.003°
γ
90°
Cell volume
2625 ± 0.6 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
7
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.1243
Residual factor for significantly intense reflections
0.0959
Weighted residual factors for significantly intense reflections
0.1528
Weighted residual factors for all reflections included in the refinement
0.1627
Goodness-of-fit parameter for all reflections included in the refinement
