Stereoselective synthesis of functionalized perhydropyrrolo[1,2-b]isoxazoles based on (3+2)-annulation of donor-acceptor cyclopropanes and isoxazolines
Authors of publication
Potapov, Konstantin V.; Novikov, Maxim A.; Kozmenko, Yaroslav V.; Solyev, Pavel N.; Volodin, Alexander D.; Korlyukov, Alexander; Novikov, Roman A.; Tomilov, Yury
Journal of publication
Organic & Biomolecular Chemistry
Year of publication
2025
a
10.6316 ± 0.0014 Å
b
14.5653 ± 0.0019 Å
c
12.9547 ± 0.0017 Å
α
90°
β
91.98 ± 0.004°
γ
90°
Cell volume
2004.9 ± 0.5 Å3
Cell temperature
120 K
Ambient diffraction temperature
120 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0519
Residual factor for significantly intense reflections
0.0386
Weighted residual factors for significantly intense reflections
0.1013
Weighted residual factors for all reflections included in the refinement
0.107
Goodness-of-fit parameter for all reflections included in the refinement
