Stereoselective synthesis of functionalized perhydropyrrolo[1,2-b]isoxazoles based on (3+2)-annulation of donor-acceptor cyclopropanes and isoxazolines
Authors of publication
Potapov, Konstantin V.; Novikov, Maxim A.; Kozmenko, Yaroslav V.; Solyev, Pavel N.; Volodin, Alexander D.; Korlyukov, Alexander; Novikov, Roman A.; Tomilov, Yury
Journal of publication
Organic & Biomolecular Chemistry
Year of publication
2025
a
8.598 ± 0.006 Å
b
10.18 ± 0.006 Å
c
12.966 ± 0.012 Å
α
71.3 ± 0.03°
β
80.52 ± 0.03°
γ
76.2 ± 0.03°
Cell volume
1039.1 ± 1.4 Å3
Cell temperature
120 K
Ambient diffraction temperature
120 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.104
Residual factor for significantly intense reflections
0.058
Weighted residual factors for significantly intense reflections
0.1372
Weighted residual factors for all reflections included in the refinement
0.1544
Goodness-of-fit parameter for all reflections included in the refinement
