Information card for entry 7204621

Structure parameters

• Formula: C18 H54 B20 N2 O19 W5
• Calculated formula: C18 H54 B20 N2 O19 W5
• Title of publication: The 'globule‒globule' hybrid dicarbaborane‒polyoxometallate salt, [C2B10H11CH2NHCH(CH3)2]4[W10O32][H2O]2[(CH3)2CO]4
• Authors of publication: Macías, Ramón; Kennedy, John D.; Thornton-Pett, Mark; Román, Pascual
• Journal of publication: CrystEngComm
• Year of publication: 2003
• Journal volume: 5
• Journal issue: 19
• Pages of publication: 93
• a: 11.5428 ± 0.0002 Å
• b: 12.485 ± 0.0002 Å
• c: 18.4962 ± 0.0003 Å
• α: 97.196 ± 0.0006°
• β: 106.027 ± 0.0006°
• γ: 107.916 ± 0.0006°
• Cell volume: 2372.42 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0399
• Residual factor for significantly intense reflections: 0.0369
• Weighted residual factors for significantly intense reflections: 0.0949
• Weighted residual factors for all reflections included in the refinement: 0.098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No