Information card for entry 7204622

Structure parameters

• Formula: C29 H32 Cl2 Fe N6 Ni O16.5
• Calculated formula: C29 H30 Cl2 Fe N6 Ni O16.5
• Title of publication: Controlling the construction of trinuclear, 1-D, and 2-D Ni(ii)Fe(ii)/Fe(ii)Fe(ii) complexes: selective syntheses, structures, and magnetic properties
• Authors of publication: Kamiyama, Asako; Noguchi, Tomoko; Kajiwara, Takashi; Ito, Tasuku
• Journal of publication: CrystEngComm
• Year of publication: 2003
• Journal volume: 5
• Journal issue: 40
• Pages of publication: 231
• a: 10.1635 ± 0.0016 Å
• b: 19.999 ± 0.003 Å
• c: 20.833 ± 0.003 Å
• α: 90°
• β: 103.159 ± 0.003°
• γ: 90°
• Cell volume: 4123.3 ± 1.1 ų
• Cell temperature: 220 ± 2 K
• Ambient diffraction temperature: 220 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2003
• Residual factor for significantly intense reflections: 0.0733
• Weighted residual factors for significantly intense reflections: 0.1789
• Weighted residual factors for all reflections included in the refinement: 0.2366
• Goodness-of-fit parameter for all reflections included in the refinement: 0.877
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No