Information card for entry 7219349

Structure parameters

• Formula: C79 H73 Ir2 N9 O15 Pb
• Calculated formula: C79 H73 Ir2 N9 O15 Pb
• Title of publication: Four new lead(ii)‒iridium(iii) heterobimetallic coordination frameworks: synthesis, structures, luminescence and oxygen-sensing properties
• Authors of publication: Chen, Yi-Ting; Lin, Chun-Yen; Lee, Gene-Hsiang; Ho, Mei-Lin
• Journal of publication: CrystEngComm
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 10
• Pages of publication: 2129
• a: 13.0965 ± 0.0002 Å
• b: 16.9698 ± 0.0003 Å
• c: 19.3066 ± 0.0003 Å
• α: 67.1073 ± 0.0009°
• β: 71.2175 ± 0.001°
• γ: 88.2966 ± 0.001°
• Cell volume: 3719.82 ± 0.11 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0891
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1181
• Weighted residual factors for all reflections included in the refinement: 0.135
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No