Information card for entry 7219350

Structure parameters

• Formula: C142 H122 I4 Ir4 N18 O28 Pb4
• Calculated formula: C142 H118 I4 Ir4 N18 O28 Pb4
• Title of publication: Four new lead(ii)‒iridium(iii) heterobimetallic coordination frameworks: synthesis, structures, luminescence and oxygen-sensing properties
• Authors of publication: Chen, Yi-Ting; Lin, Chun-Yen; Lee, Gene-Hsiang; Ho, Mei-Lin
• Journal of publication: CrystEngComm
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 10
• Pages of publication: 2129
• a: 8.7126 ± 0.0002 Å
• b: 18.2978 ± 0.0004 Å
• c: 22.6191 ± 0.0005 Å
• α: 87.0367 ± 0.0009°
• β: 83.5709 ± 0.0009°
• γ: 79.003 ± 0.001°
• Cell volume: 3515.79 ± 0.14 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0849
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.0925
• Weighted residual factors for all reflections included in the refinement: 0.1119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No