Information card for entry 7235282

Structure parameters

• Formula: C130 H104 Cl2 N29.5 Ni7 O24.75
• Calculated formula: C130 H102.5 Cl2 N29.5 Ni7 O24.75
• Title of publication: An indeno-quinoxaline based oxime ligand for the synthesis of polynuclear Ni(ii) clusters
• Authors of publication: Canaj, Angelos B.; Nodaraki, Lydia E.; Philippidis, Aggelos; Tzimopoulos, Demetrios I.; Fotopoulou, Eirini; Siczek, Milosz; Lis, Tadeusz; Milios, Constantinos J.
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 32
• Pages of publication: 13214
• a: 18.314 ± 0.007 Å
• b: 18.903 ± 0.006 Å
• c: 19.287 ± 0.006 Å
• α: 96.06 ± 0.03°
• β: 106.28 ± 0.03°
• γ: 101.89 ± 0.03°
• Cell volume: 6176 ± 4 ų
• Cell temperature: 80 ± 2 K
• Ambient diffraction temperature: 80 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2127
• Residual factor for significantly intense reflections: 0.0901
• Weighted residual factors for significantly intense reflections: 0.1474
• Weighted residual factors for all reflections included in the refinement: 0.1914
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No