Information card for entry 7235283

Structure parameters

• Formula: C135.75 H108.4 Cl2 N27 Ni8 O29.95
• Calculated formula: C135.75 H108 Cl2 N27 Ni8 O29.95
• Title of publication: An indeno-quinoxaline based oxime ligand for the synthesis of polynuclear Ni(ii) clusters
• Authors of publication: Canaj, Angelos B.; Nodaraki, Lydia E.; Philippidis, Aggelos; Tzimopoulos, Demetrios I.; Fotopoulou, Eirini; Siczek, Milosz; Lis, Tadeusz; Milios, Constantinos J.
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 32
• Pages of publication: 13214
• a: 17.608 ± 0.005 Å
• b: 18.43 ± 0.005 Å
• c: 21.084 ± 0.006 Å
• α: 81.07 ± 0.03°
• β: 82.32 ± 0.03°
• γ: 83.47 ± 0.03°
• Cell volume: 6668 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.174
• Residual factor for significantly intense reflections: 0.0613
• Weighted residual factors for significantly intense reflections: 0.0903
• Weighted residual factors for all reflections included in the refinement: 0.1021
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No