Crystallography Open Database

Information card for entry 7700122

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Coordinates	7700122.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H39 Ga P2
Calculated formula	C40 H39 Ga P2
Title of publication	Reactivity of the carbodiphosphorane, (Ph<sub>3</sub>P)<sub>2</sub>C, towards main group metal alkyl compounds: coordination and cyclometalation.
Authors of publication	Quinlivan, Patrick J.; Shlian, Daniel G.; Amemiya, Erika; Parkin, Gerard
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	25
Pages of publication	9139 - 9151
a	16.0714 ± 0.0006 Å
b	11.5306 ± 0.0004 Å
c	18.5845 ± 0.0007 Å
α	90°
β	109.839 ± 0.0005°
γ	90°
Cell volume	3239.6 ± 0.2 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0529
Residual factor for significantly intense reflections	0.0447
Weighted residual factors for significantly intense reflections	0.1381
Weighted residual factors for all reflections included in the refinement	0.1413
Goodness-of-fit parameter for all reflections included in the refinement	1.622
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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