Conversion of some substituted phenols to the corresponding masked thiophenols, synthesis of a dinickel(II) dithiolate macrocyclic complex and isolation of some metal- and ligand-based oxidation products
Authors of publication
Brooker, Sally; Caygill, Graham B.; Croucher, Paul D.; Davidson, Tony C.; Clive, Derrick L. J.; Magnuson, Stephen R.; Cramer, Stephen P.; Ralston, Corie Y.
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
2000
Journal issue
18
Pages of publication
3113
a
11.854 ± 0.007 Å
b
15.45 ± 0.007 Å
c
25.559 ± 0.014 Å
α
90°
β
91.291 ± 0.01°
γ
90°
Cell volume
4680 ± 4 Å3
Cell temperature
183 ± 2 K
Ambient diffraction temperature
183 ± 2 K
Number of distinct elements
5
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.1144
Residual factor for significantly intense reflections
0.0645
Weighted residual factors for significantly intense reflections
0.1587
Weighted residual factors for all reflections included in the refinement
0.1854
Goodness-of-fit parameter for all reflections included in the refinement
