Conversion of some substituted phenols to the corresponding masked thiophenols, synthesis of a dinickel(II) dithiolate macrocyclic complex and isolation of some metal- and ligand-based oxidation products
Authors of publication
Brooker, Sally; Caygill, Graham B.; Croucher, Paul D.; Davidson, Tony C.; Clive, Derrick L. J.; Magnuson, Stephen R.; Cramer, Stephen P.; Ralston, Corie Y.
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
2000
Journal issue
18
Pages of publication
3113
a
8.9104 ± 0.0019 Å
b
9.1521 ± 0.0019 Å
c
12.172 ± 0.003 Å
α
70.605 ± 0.003°
β
85.336 ± 0.003°
γ
68.074 ± 0.003°
Cell volume
867.5 ± 0.3 Å3
Cell temperature
168 ± 2 K
Ambient diffraction temperature
168 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0346
Residual factor for significantly intense reflections
0.0284
Weighted residual factors for significantly intense reflections
0.0692
Weighted residual factors for all reflections included in the refinement
0.0715
Goodness-of-fit parameter for all reflections included in the refinement
