Information card for entry 7704310

Structure parameters

• Formula: C50 H80.06 Br0.94 Ge N2 O4.06 S2 Si4
• Calculated formula: C50 H80.06 Br0.94 Ge N2 O4.06 S2 Si4
• Title of publication: 1,2-Insertion reactions of alkynes into Ge-C bonds of arylbromogermylene.
• Authors of publication: Sugahara, Tomohiro; Espinosa Ferao, Arturo; Rey Planells, Alicia; Guo, Jing-Dong; Aoyama, Shin; Igawa, Kazunobu; Tomooka, Katsuhiko; Sasamori, Takahiro; Hashizume, Daisuke; Nagase, Shigeru; Tokitoh, Norihiro
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 21
• Pages of publication: 7189 - 7196
• a: 10.7385 ± 0.0001 Å
• b: 20.7088 ± 0.0002 Å
• c: 26.3913 ± 0.0003 Å
• α: 76.872 ± 0.001°
• β: 88.089 ± 0.001°
• γ: 78.773 ± 0.001°
• Cell volume: 5605.81 ± 0.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0598
• Residual factor for significantly intense reflections: 0.0381
• Weighted residual factors for significantly intense reflections: 0.0819
• Weighted residual factors for all reflections included in the refinement: 0.0893
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No