Information card for entry 7704309

Structure parameters

• Formula: C30 H59 Br Si5
• Calculated formula: C30 H59 Br Si5
• SMILES: Br[Si]1(c2c(C([Si](C)(C)C)[Si](C)(C)C)cc(cc2C([Si](C)(C)C)[Si](C)(C)C)C(C)(C)C)C(=C1CC)CC
• Title of publication: 1,2-Insertion reactions of alkynes into Ge-C bonds of arylbromogermylene.
• Authors of publication: Sugahara, Tomohiro; Espinosa Ferao, Arturo; Rey Planells, Alicia; Guo, Jing-Dong; Aoyama, Shin; Igawa, Kazunobu; Tomooka, Katsuhiko; Sasamori, Takahiro; Hashizume, Daisuke; Nagase, Shigeru; Tokitoh, Norihiro
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 21
• Pages of publication: 7189 - 7196
• a: 10.1417 ± 0.0002 Å
• b: 16.7487 ± 0.0003 Å
• c: 22.3189 ± 0.0004 Å
• α: 90°
• β: 92.75 ± 0.002°
• γ: 90°
• Cell volume: 3786.73 ± 0.12 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0482
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.091
• Weighted residual factors for all reflections included in the refinement: 0.0956
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No