Crystallography Open Database

Information card for entry 7705614

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Coordinates	7705614.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C128 H192 B8 F32 N16 Pd4 Si16
Calculated formula	C128 H192 B8 F32 N16 Pd4 Si16
Title of publication	Flexibility and anion exchange of [(X)@Pd<sub>2</sub>L<sub>4</sub>] cages for recognition of size and charge of polyatomic anions.
Authors of publication	Lee, Jeyeong; Lim, Sangwoo; Kim, Dongwon; Jung, Ok-Sang; Lee, Young-A
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	42
Pages of publication	15002 - 15008
a	16.927 ± 0.003 Å
b	20.121 ± 0.004 Å
c	55.331 ± 0.011 Å
α	90°
β	90°
γ	90°
Cell volume	18845 ± 6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	70
Hermann-Mauguin space group symbol	F d d d :2
Hall space group symbol	-F 2uv 2vw
Residual factor for all reflections	0.1583
Residual factor for significantly intense reflections	0.1026
Weighted residual factors for significantly intense reflections	0.255
Weighted residual factors for all reflections included in the refinement	0.2861
Goodness-of-fit parameter for all reflections included in the refinement	1.157
Diffraction radiation wavelength	0.8 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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