Information card for entry 7705615

Structure parameters

• Formula: C65 H100 N8 O13 Pd2 Re3 Si8
• Calculated formula: C65 H100 N8 O13 Pd2 Re3 Si8
• Title of publication: Flexibility and anion exchange of [(X)@Pd₂L₄] cages for recognition of size and charge of polyatomic anions.
• Authors of publication: Lee, Jeyeong; Lim, Sangwoo; Kim, Dongwon; Jung, Ok-Sang; Lee, Young-A
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 42
• Pages of publication: 15002 - 15008
• a: 20.087 ± 0.004 Å
• b: 16.899 ± 0.003 Å
• c: 29.527 ± 0.006 Å
• α: 90°
• β: 109.4 ± 0.03°
• γ: 90°
• Cell volume: 9454 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1476
• Residual factor for significantly intense reflections: 0.1213
• Weighted residual factors for significantly intense reflections: 0.3244
• Weighted residual factors for all reflections included in the refinement: 0.3429
• Goodness-of-fit parameter for all reflections included in the refinement: 2.121
• Diffraction radiation wavelength: 0.7 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No